PY-GCMS6188Thermal cracking gas chromatography-mass spectrome

Product introduction:The PY-GCMS6188 thermal cracking gas phase system uses programmed temperature rise thermal analysis and high-temperature cracking. Four types of ortho benzene plasticizers controlled by ROHS2.0 are volatilized at high temperatures between 200 ° C and 450 ° C. They are then separated by gas chromatography in batches according to different temperatures, a

Product Analysis

The PY-GCMS6188 thermal cracking gas phase system uses a program to perform thermal analysis and high-temperature cracking. Four types of ortho benzene plasticizers controlled by ROHS2.0 are evaporated at high temperatures ranging from 200 ℃ to 450 ℃. They are then separated by gas chromatography in batches according to different temperatures and qualitatively and quantitatively detected by mass spectrometry.

·Short sample preparation time, with a sample preparation time of 20 minutes per sample, fully meets the rapid screening needs of enterprise users;
·Environmental Impact Assessment: No pre-treatment required, no hazardous chemical reagents, no generation of waste gas or liquid, no need to apply for environmental impact assessment;
·Personnel configuration: One operator is sufficient, who understands basic computer operations;
·Low cost of use: no pre-treatment, no need for reagents and consumables;
·Direct injection without pre-treatment: Direct solid or liquid injection without pre-treatment;
·Built in standard curve: more intuitive judgment of whether the material exceeds the limit of ortho benzene;
·Suitable for 100% polymer materials: Chemical methods are only suitable for some materials, PY-GCMS6188 is suitable for the vast majority of materials;
·No need for a professional laboratory environment: only a regular operating space with air conditioning power supply is required for installation and use.

Environmental Requirements

Environmental temperature: -5 ℃~35 ℃ Overall dimensions: 1280 * 480 * 480mm Power requirements: AC220V+10%, 50/60 Hz
Relative humidity: ≤ 85% Measurement conditions: atmospheric environment Net weight: 70Kg

Technical Specifications

Technical indicators of gas chromatograph
Split/non split injection port: Column temperature box:
Maximum operating temperature: Room temperature+7-450 ℃, controllable at any temperature point Temperature control accuracy: less than 0.1 ℃;
Pressure control range: 0-100psi Program heating order: Multi stage and multi platform program heating (column box);
Pressure control accuracy: 0.002psi Program heating rate: 120 ℃/min;
Equipped with pulse splitting and pulse non splitting injection modes Cooling rate: from 350 ℃ to 50 ℃<5 minutes;
Split ratio setting range: 1000:1 Retention time reproducibility: less than 0.002 minutes.
Control range of flow rate for gasket blowing: 0-100mL/min
Mass spectrometry technical indicators
Ion source Quality analysis
Front open cavity design allows for direct disassembly and assembly of the ion source from the front without the need to open the instrument casing Quality analyzer: high-precision metal molybdenum quadrupole with pre quadrupole, improving edge field and reducing quadrupole contamination
Ionization method: EI Quality range: 1.5-1000 amu, increasing in increments of 0.1 amu
Ionization energy (electron bombardment source EI): 5eV -250eV (commonly used 70eV) Resolution: resolution per unit mass
Ion source set temperature: 100-350 ° C continuously adjustable Quality axis stability:+0.10mu/48h
Filament: Dual filament Scanning speed: up to 1000amu/s
Fully self-developed high-performance filament, reducing maintenance costs
Range of filament emission current setting: 0-350uA
Detector
Detection system: secondary electron multiplier with focusing lens;
Detector: off-axis electron multiplier with high-energy dynode;
Sensitivity
Full scan, 1pg octafluoronaphthalene (OFN) at m/z 272
At amu, the signal-to-noise ratio (S/N) is ≥ 30:1 (RMS)
Dynamic range :10⁶
Vacuum system
Front stage pump: oil rotary vane pump, pumping speed 5m ³/h;
Molecular pump: Turbomolecular pump, pumping speed 90L/s;
Equipped with a full range cold cathode vacuum gauge, providing real-time vacuum information
Temperament interface
The maximum operating temperature of the interface is 450 ℃

PY-GCMS6188 Technical Specifications

1: The gas chromatograph adopts the advanced 10/100M adaptive Ethernet communication interface and built-in IP protocol stack, so that the instrument can easily realize long-distance Data transmission; Facilitating the setup of the laboratory, simplifying the configuration of the laboratory, and facilitating the management of analytical data;
2: Three independent connection processes are designed inside the instrument, which can be connected to local processing (laboratory site), unit supervisors (such as quality inspection department heads, production plant managers, etc.), and higher-level supervisors (such as environmental protection bureaus, technical supervision bureaus, etc.), making it convenient for unit supervisors and higher-level supervisors to monitor the operation of the instrument in real time and analyze data results;
3: The Netkrt workstation equipped with the instrument enables data processing and control, simplifies document management, and significantly reduces users' laboratory investment and operating costs;
4: The instrument can be connected to the manufacturer through the Internet to realize remote diagnosis, remote program update, etc. (with the user's permission);
5: The instrument is equipped with a 7-inch true color display screen, which displays clear, elegant color tones, and high-end atmosphere;
6: The system has two operating systems in Chinese and English, which can be freely switched;
7: The temperature control area can be freely named by users for convenient use;
8: The instrument adopts a modular structural design, which is clear in design, easy to replace and upgrade, and protects the effectiveness of investment;
9: A brand new microcomputer temperature control system with high temperature control accuracy, superior reliability and anti-interference performance; Equipped with a six channel fully independent temperature control system, it can achieve sixteen step programmed temperature rise, enabling the device to handle a wider range of sample analysis;
Equipped with a column box automatic rear door opening system, the precision of low-temperature control is improved, and the speed of temperature rise/fall is faster;
10: The instrument is equipped with advanced electronic flow controllers (EFC) and electronic pressure controllers (EPC) to achieve digital control of the carrier gas and chromatographic column gas path, which can greatly improve the stability and reproducibility of quantitative results;
11: The chromatography machine is equipped with a low-noise, high-resolution 24 bit AD circuit and has the functions of baseline storage and baseline subtraction;
12: The randomly equipped workstation is suitable for operating systems such as Win11, Win7, Win10 in both Chinese and English;
13: The chromatographic system has a standard interface of MODBUS/TCP, which can be easily integrated with DCS.
14: Main features: (1) 8-way heating system, (2) 10 file libraries, (3) 30 level programmed temperature rise column box, (4) 7-inch true color screen display function, easy to operate, switchable between Chinese and English, (5) multiple program functions, ignition, memory Self diagnosis, time program, automatic rear door opening, return control function, remote operation of various parameters, and ten work file operation functions (6). Multiple detector selection and configuration functions (FID, TCD, FPD, ECD).

PY-GCMS6188 Thermal Cracking Gas Chromatography Mass Spectrometry Application Fields

Electronics and Electrical Petrochemical Plastic Plastic
Electrical industry Automotive industry Packaging/Printing

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